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By Samuel Zalipsky, Jane L. Chang, Fernando Albericio, George Barany

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Extra resources for Preparation and applications of polyethylene glycol-polystyrene graft resin supports for solid-phase peptide synthesis

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3 cm h e a v i l y s h i e l d e d Nal ( T l ) detector w i t h a 1 cm opening i n the c o l l i m a t o r was placed 20 cm from the o u t l e t of the gener­ a t o r . T h i s o u t l e t was connected to the intravenous tubing i n s e r t e d i n t o an a n t e c u b i t a l v e i n of the p a t i e n t . The de­ t e c t o r was connected to a spectrometer set at 260 keV w i t h a 10% window. Three-second measurements were performed im­ mediately a f t e r e l u t i o n i n groups of 6 e l u t i o n s repeated every 3 min i n each p a t i e n t .

Ch003 3. ; ACS Symposium Series; American Chemical Society: Washington, DC, 1984. ; ACS Symposium Series; American Chemical Society: Washington, DC, 1984. BETT ETAL. ch003 3. ; ACS Symposium Series; American Chemical Society: Washington, DC, 1984. ch003 42 Time after activity absorbed on columns ( hours ) Figure 4. CPG Lipoamide Columns: Time dependence of e l u t i o n e f f i c i e n c y f o r d i f f e r e n t " s p e c i f i c a c t i v i t y " columns. ; ACS Symposium Series; American Chemical Society: Washington, DC, 1984.

H. Coleman i n the e a r l y stages of t h i s work, and a l s o D. L. Stone, P. L. Evans and D. Cooper - students who have a l l contributed g r e a t l y to t h i s work. F i n a l l y our thanks are due t o the V a r i a b l e Energy C y c l o t r o n s t a f f f o r providing proton beams on demand and f o r manufacture of targets and other apparatus. Literature Cited 1. J. Br. Heart J o u r n a l 1979, 41, 68-78. 2. C. B r . J. R a d i o l . 1969, 42,237. 3. A. J . Nucl. Med. 1980, 21,1169-1176.

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