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By Gunter Zweig and Joseph Sherma (Eds.)

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_ 1. RESIDUE ANALYSIS BY MASS SPECTROMETRY 29 Relative intensity Relative intensity— CI 'I 30 " i 40 1 i 50 1 60 1 70 1 — " 80 m/e — 1 i 380 390 4 0 0 1 410 FIG. 18. Electron ionization and field desorption mass spectra of 1,4,5,6,7,7hexachloro-5-norbornene-2,3-en(io-dicarboxycylic acid [Schulten and Beckey (1973a). ] A n u m b e r of organochlorine pesticides h a v e b e e n e x a m i n e d using field d e s o r p t i o n m a s s spectral t e c h n i q u e s . S c h u l t e n a n d B e c k e y (1973a) h a v e published F D m a s s s p e c t r a of a n u m b e r of organochlorine c o m p o u n d s , a m o n g t h e m the dicarboxycylic acid s h o w n in Fig.

J. Agric. Food Chem. 18, 405. Plimmer, J. , Ruth, J. , and Woolson, E. A. (1973). J. Agric. Food Chem. 21, 90-93. Rote, J. , and Morris, W. J. (1973). J. Assoc. Off. Anal. Chem. 56, 188-199. Ryan, J. , Biros, F. , and Harless, R. L. (1974). 22nd Annu. Conf Mass Spectrom. , Am. Soc. , 1974 No. C-2. Ryan, J. , Harless, R. , and Lewis, R. G. (1975). 23rd Annu. Conf Mass Spectrom. , 1975. Paper No. A l l . , and Hutzinger, O. (1973). ' CRC Press, Cleveland, Ohio. Schoengold, D. , and Munson, M. S. B.

1974) reported e v i d e n c e of c o n t a m i n a t i o n of hexa c h l o r o b e n z e n e ( H C B ) with significant quantities of heptachloro- and octachlorodibenzodioxins a n d h e p t a c h l o r o - and octachlorofurans. Confirmation w a s carried out using normal G C - M S t e c h n i q u e s . 9 p p m . A s in previous w o r k d i s c u s s e d , identities w e r e confirmed by G C - M S . B a u g h m a n (1974) discussed the various w a y s by which chlorodioxins could be introduced into the e n v i r o n m e n t .

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